EMS MATERIALS SCIENCE & METROLOGY CATALOG 2019–20 EDITION TEM SUPPLIES


Wet “Liquid” TEM Kit


Why K-Kit?


K-kit Meets All Needs for Liquid TEM


1 Native State in Liquid • Available with undiluted solution.


• Preserve the original morphology and physical state in liquid 2 In-situ Observation


• Kinetic mechanism of metal growth or physicochemical reaction process in liquid can be in-situ observed with increased reaction time.


3 Quantitative Analysis


• Software of image recognition for nanoparticle size distribution analysis.


4 Compatible with Versatile Microscopy Analyses


• Applicable to TEM, FIB, and STEM. • Available for EDX analysis. • High resistance to most chemicals.


• Working temperature range from -40°C to 120°C.


Patents being issued and publication:


US 7807979 B2 US 8969827 B2


Anal. Chem.2012, 84: 6312-6316


 K-Kit A Specimen Holder for Liquid Sample Analysis in TEM


OVERVIEW


K-kits are sample holders designed to facilitate convenient TEM observation of liquid samples, allowing nano-objects, aggregates, and agglomerates (NOAAs) in liquid samples to be characterized.


With vacuum compatible sealing of liquids in electron-transmitting thickness, K-kits are micro reaction chambers for countless experiments in materials, chemical, and biological research.


FEATURES • Applicable for most TEM holder brands


• Strong structural reliability under vacuum • Sealing glue compatible to many solvents • Disposable • Free of cross-contamination • Easy to use


Sample Analysis Comparison K-kit original physical state


K-Kit Die Grid Step Cap Seal K-Kit Stand Base


K-Kit Carrier


Conventional aggregated after drying K-Kit


Images shown: NIST traceable polystyrene beads. Scale Bar 500nm.


Dimensions Window Length:


300µm, Width 25µm


Channel Height (H): 0.2 and 2.0 standard 0.5, 1.0 and 5.0 available


H = 0.2µm, 0.5µm, 1µm, 2µm, 5µm


84


Physicochemical Parameters Composition Size


Shape Size Distribution


Aggregation and Agglomeration in liquid Particle Concentration Liquid TEM Observation


K-kit       


Cu-Grid    ∆ X X X


= Good ∆ = Case Dependent X = Not Available


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