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62 SILICONES


containing 1% Polyquaternium-7 (Figure 3). The silky, shine, softness, hair gloss, healthy


looking, ease of combing were not much different. The application of Nano Olive Oil in shampoo production can partially replace Polyquaternium-7 but make a big difference in the feeling of strong hair.


Test 4: Comb force test To evaluate the difference in brushing force between the shampoo containing 1% Polyquaternium-7 and the shampoo containing a mix of 3% Nano Olive Oil and 0.5% Polyquaternium-7, the combing force was measured before and after treatment; for wet hair and dry hair.


Results


The shampoo containing a mix of 0.5% Polyquaternium-7 + 3% Nano Olive Oil reduced wet comb force by 25% and dry comb force by 35% compared to shampoo containing 1% Polyquaternium-7 (Figure 4).


Test 5: Hair shine test Naturally straight, black hair tresses were treated with shampoo containing 1% Polyquaternium-7 or shampoo containing a mix of 3% Nano Olive Oil and 0.5% Polyquaternium-7. Hair gloss measurements were taken before and after shampoo treatment, with and without heat.


Results Shampoo containing a mix of 3% Nano Olive Oil and 0.5% Polyquaternium-7 resulted in statistically significant (p <0.05) increases in hair shine compared to shampoo containing 1% Polyquaternium-7 with and without heat (Figure 5).


Test 6: Curl retention test Curl hair tresses were treated with shampoo containing 1% Polyquaternium-7 or shampoo containing a mix of 3% Nano Olive Oil and 0.5% Polyquaternium-7. The increase in the area of the tress along the time indicates that the curls lost their initial shape.


Results Shampoo containing a mix of 3% Nano Olive Oil and 0.5% Polyquaternium-7 showed a significant efficacy in holding of curls (small-area variation) up to 24 hours compared to shampoo containing 1% Polyquaternium-7 (Figure 6).


Shampoo containing 1% polyquaternium ■ Shampoo containing 0.5% polyquaternium


+ 3% Nano olive oil ■


100 80 60 40 20 0


-20 -40 -60


Wet Comb Force


DryComb Force


Figure 4: Reduction in comb force PERSONAL CARE November 2022 Ease of Combing*


TEST 2: Samples


A B C


40 30 20 10 0


Contents


C + 3% Nano Olive Oil C + 3% dimethicone Shampoo contents


26.504 25.973 24.079


A ■ B■ C■ 31.976


29.589 31.536 Before use After use


40 30 20 10 0


Remarks Test group


Positive control group Negative control group


A ■ B■ C■ 35.469


21.435 14.392


Rate of change (%) = (after-before)/before*100 Figure 2: Hair friction and rate of change between sample A, sample B and sample C Overall Product Performance


100% 80% 60% 40% 20%


Hair Strength** Smoothness**


Healthy Looking**


Softness** Silky Figure 3: Sensorial analysis


Test 7: Surface characterization test by SEM The study was conducted to show the effectiveness of repairing damaged hair on the surface between two groups: using a shampoo containing Nano Olive Oil and using a regular shampoo after one wash. Hair surface images were taken by SEM (scanning electron microscopy).


0.5% Polyquaternium-7 + 3% Micellium Oils SIL-1501 HA ■ 1% Polyquaternium-7 ■


80 60 40 20 0


-20 With heat Figure 5: Hair shine Figure 6: Curl retention www.personalcaremagazine.com No Heat


40 30 20 10 0


Results Shampoo containing Nano Olive Oil showed morphological improvement in cuticle integrity (less damage) and smoothness compared to untreated (Figure 7).


Test 8: Split ends protection test This study was conducted to prove the effectiveness of repairing split ends between


0.5% Polyquaternium-7 + 3% Micellium Oils SIL-1501 HA ■ 1% Polyquaternium-7 ■


Shine** 1% Polyquaternium-7 ■ 0.5% Polyquaternium-7 + 3% Nano Olive Oil ■


4


12 Time (hours)


24


Percent reduction Comb Force (%)


Percent change in Hair Shine (relative to untreated hair) (%)


BNT


Tress area variation


%


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