90 FORMULATIONS
Add the mix E under emulsifier 1500rpm, 10 minutes. Heat A to 75°C. Emulsify A inti BCDE under emulsifier 2500rpm, 10 minutes. Cool down to 35°C under gentle agitation. Add F materials under gentle agitation for 20 minutes. Check the pH. Suppliers 1 Gattefosse 2 A.M.I. 3 Stearinerie Dubois 4 Olisud 5 Quimasso 6 Thor 7 Quaron 8 IMCD 9 LCW 10 Codif Technologie Naturelle 11 Schülke & Mayr
DUPONT Great Tasting SLS-free Gel Toothpaste PHASE INGREDIENTS A
INCI NAME
CMC Cekol® Zemea®
Propanediol2 Splenda®3
Peppermint Oil4 Water
B C D Zemea®
Propanediol2 SorbogemTM5 Zeodent® Zeodent® Lathanol®
1166 1656 LAL7
20001
Cellulose Gum Propanediol
Sucralose Mentha Piperita Oil Propanediol Sorbitol
Zeodent 116 Zeodent 165
Sodium Lauryl Sulfoacetate
Appearance: Off-white yellowish cream Suppliers 1 Lucas Meyer 2 Elementis 3 Croda 4 Nusil 5 Dow Corning 6 Merck 7 SLI Chemical
GATTEFOSSÉ Refresh & Protect Bi-Gel SPF30 PHASE INGREDIENTS A1 Demineralized
INCI NAME Water
% W/W 1.00 4.00
0.20 0.75
22.75 25.00
20.30 23.00 2.50 0.50
Procedure Mix together Phase A until homogenous, homogenize if necessary. Add Phase A to Phase B. Dry mix Phase C and add to AB. Homogenize mixture until smooth. Add Phase D and mix until fully incorporated. Suppliers 1 CP Kelco 2 DuPont Tate & Lyle Bio Products 3 Sweet Solutions 4 Kerry 5 Ingredion 6 Huber 7 Stepan
ELEMENTIS Busy Bee Eye Defender PHASE INGREDIENTS/INCI NAME A
Deionized Water Glycerin
B
Water (and) Sea Salt Extract (and) Propanediol (and) Phospholipids (and) Stearoyl Inulin (Detoxium)1 Caprylic/Capric Triglyceride (and) Stearalkonium Hectorite (and) Propylene Carbonate (Bentone Gel® Isododecane (Fancol®
ID-CG)2
Caprylic/Capric Triglyceride (Crodamol GTCC)3 Phenyl Trimethicone (CPF-3300, 20cst)4 Cetyl Diglyceryl Tris (Trimethylsiloxy)silylethyl
Dimethicone (Dow Corniing 5600 Silicone Glycerol Emulsifier)5 Cyclopentasiloxane (and) Dimethicone
Crosspolymer (Dow Corning 9040 Silicone Elastomer Blend)5 Simmondsia Chinensis Seed Oil (Jojoba Oil)
Propylene Glycol (and) BHT (and) Ascorbyl Palmitate (and) Glyceryl Stearate (And) Citric Acid (Oxynex 2004)6
C Mica6 D Glycerin (and) Water (and) Dextran (and)
Caprooyl-Tetrapeptide-3 (Chronoline)1 Potassium Sorbate (and) Sodium Benzoate (and) Benzyl Alcohol (and) Aqua (Sharonmix 703)7
Water Carbopol®
A2 Aqua Acrylates Copolymer SF-1 OS Polymer
Satiaxane™ CX91 Xanthan Gum Glycerin
Glycerin
A3 E.D.T.A. Disodium Disodium Edta Salt
A4 B
Sodium Hydroxide Water, Sodium Hydroxide (10 % SOL.)
Emulfree® CBG Acticire® MB
Isostearyl Alcohol, Butylene Glycol Cocoate, Ethylcellulose Jojoba Esters, Helianthus
Annuus (Sunflower) Seed Wax, Acacia Decurrens Flower Wax, Polyglycerin-3
Schercemol™ Dis Diisopropyl Sebacate
Ester Hallbrite®
BHB
Cocoate™ BG Parsol®
1789 Uvinul® A PLUS Tinosorb®
F-2012-02 % W/W
62.30 7.00 2.00
5.50 GTCC V)2
5.00 5.00 3.00 3.00
2.00
2.00 0.20
1.00 1.00
1.00
Procedure Mix Phase A and heat to 50°C. Heat Phase B to 50°C. Add Phase C to Phase B and homogenize for several minutes. Add Phase A to Phase B/C and continue homogenizing with lower shear. Cool to below 40°C with propeller mixing and add Phase D. Properties Viscosity: DV-II, Spindle 6, 20 rpm, 7500cp
PERSONAL CARE NORTH AMERICA E F
C D
Parsol® Parsol® Parsol®
S
MCX EHS 340
Tinogard®
Water Parsol®
TL Preservative Demineralized HS
Parfum Dome Relax
Procedure Mix water + Carbopol®
Butyl Octyl Salycilate Butylene Glycol Cocoate
Butyl Methoxydibenzoylmethane Diethylamino Hydroxybenzoyl Hexyl Benzoate
BIS-Ethylhexyloxyphenol Methoxyphenyl Triazine
Ethylhexyl Methoxycinnamate Ethylhexyl Salicylate Octocrylene
Benzotriazolyl Dodecyl P-Cresol Preservative Water
Phenylbenzimidazole Sulfonic Acid
Sodium Hydroxide Water, Sodium Hydroxide (10 % SOL.)
Fragrance
Sodium Hydroxide Water, Sodium Hydroxide (10 % SOL.)
dispersed right before introduction in A1) and mix for 5 minutes (600-800 rpm). Then add A3 and mix for 5 minutes until complete solubilization of EDTA. Then add A4 to neutralize partially Carbopol®
5.00
3.00 3.00 3.00 0.50
3.00
2.00 5.00 5.00 1.00 0.70 6.00
3.00 4.00
0.30 1.15 Aqua SF1-OS at room temperature. Then add A2 (pre- Aqua SF1-OS. Heat B up
to 80 °C until complete solubization. Add slowly B (75 °C) to A (75°C) under mixing (1500 rpm) for 15 minutes. Cool under high shear (1200 rpm) for 30 minutes to 40 °C. Then add C under mixing (600 rpm). Premix D until complete solubilization of Parsol®
rpm) for 1minute. Cool under mixing to 30-35 °C. Then add E under mixing (600 rpm) for 1 minute. Add F to adjust pH above 7.2. Complete cooling to 25-27 °C under mixing (600 rpm). Properties Aspect: Glossy and slightly yellow fluid emulsion pH = 7.3 ± 0.3 Viscosity Brookfield RV (spindle A, speed 5): approx. 5 000 mPa.s after 24h SPF in vivo (ISO 24 444): 35 (5 subjects) UVA in vitro (ISO 24 443): 19 Water-resistance in vivo (Colipa 2005): 61.2% (5 subjects)
May 2020 HS and add to batch under mixing (600-800
0.10 3.00 0.10
0.50 5.00 1.00
1641-2.04 % W/W
41.65 3.00
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