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Sample Preparation of Nanocomposites and Nanomaterials by Ultramicrotomy Leica EM UC7


a Alternative


Join us at the EMS Microscopy Academy and learn the latest techniques to reveal internal structures of composites and polymers being investigated with transmission electron microscopy (TEM) and scanning transmission electron microscopy (STEM).


Sample preparation workflow will be illustrated using the Leica EM UC7 Ultramicrotome, its EM FC7 Cryochamber, and the RMC PowerTome Ultramicrotome. Differences between FIB (Focussed Ion Beam) and ultramicrotomy samples will also be covered.


Who can benefit from


this alternative?  Composite and polymer research companies - especially from the automotive and aviation industries


 Materials scientists already working with ultramicrotomy


 FIB users preparing TEM lamellas


For more information, or to sign up for a workshop, please visit our website...


www.emsdiasum.com


P.O. Box 550 • 1560 Industry Rd. Hatfield, Pa 19440 Tel: (215) 412-8390 Fax: (215) 412-8450 email: sgkcck@aol.com


EMS Microscopy Academy


P.O. Box 550 • 1560 Industry Rd. • Hatfield, Pa 19440 Tel: (215) 412-8400 • Fax: (215) 412-8450 Toll Free: 800-523-5874 • email: sgkcck@aol.com


Mert Kurttepeli, Sara Bals, EMAT Antwerpen


[110]


Tom Willhammar, Sara Bals, EMAT Antwerpen


Applications...


Zeolite USY30 Crystal morphology STEM analysis


The mesopores (2-50 nm) and the crystalline micro-pores (0.7 nm) are clearly visualized.


Epoxy loaded with amino-functionalized CNTs TEM analysis


Powerful toFIB


DiATOME trimtool Trimming of epoxy and acrylic embeddings, polymers and non-ferrous metals


Equipment used in this Technique...


RMC PowerTome Ultramicrotomes


Leica EM UC7


DiATOME cryo sectioning of cryo-protected specimens, frozen hydrated specimens and industrial samples such as polymers and rubber.


DiATOME ultra AFM Surface sectioning for AFM investigation


DiATOME ultra sonic Rigid polymers such as PS, PMMA, ABS, HIPS, modified PP, etc.


Good preservation of the interphase Gravitational stroke!


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