Preparation of Particles for Full-Range Tomography 1157
ARSLAN, I., TONG, J.R. &MIDGLEY, P.A. (2006). Reducing the missing wedge: High-resolution dual axis tomography of inorganic materials. Ultramicroscopy 106, 994–1000.
BARNARD,D.P., TURNER,J.N., FRANK,J.&MCEWEN,B.F.(1992). A 360° single-axis tilt stage for the high-voltage electron microscope. JMicrosc 167,39–48.
BATENBURG, K.J., BALS, S., SIJBERS, J., KÜBEL, C., MIDGLEY, P.A., HERNANDEZ, J.C., KAISER, U., ENCINA, E.R., CORONADO, E.A. & VAN TENDELOO, G. (2009). 3D imaging of nanomaterials by discrete tomography. Ultramicroscopy 109, 730–740.
BIERMANS,E.,MOLINA,L., BATENBURG,K.J., BALS,S.&VAN TENDELOO,G. (2010). Measuring porosity at the nanoscale by quantitative electron tomography. Nano Letters 10, 5014–5019.
DAHMEN, T., TRAMPERT,P. & JONGE, N. De (2017). Advanced recording schemes for electron tomography. MRS Bulletin 41, 537–541.
GORIS, B., VAN DEN BROEK, W., BATENBURG, K. J., HEIDARIMEZERJI,H. &BALS, S. (2012). Electron tomography based on a total variation minimization reconstruction technique. Ultra- microscopy 113, 120–130.
HERNÁNDEZ-SAZ, J., HERRERA,M.&MOLINA, S.I. (2014). Fabrication of needle-shaped specimens containing subsurface nanostructures forelectrontomography.
In FIB Nanostructures, vol. 20,
Wang, Z.M. (Ed.), pp. 241–266. Cham: Springer Science & Business Media.
ITO, T., MATSUWAKI, U., OTSUKA, Y., HATTA, M., HAYAKAWA, K., MATSUTANI, K., TADA,T. & JINNAI, H. (2011). Three-dimensional spatial distributions of Pt catalyst nanoparticles on carbon substrates in PEM. Electrochem Commun 31, 412–421.
ITO, T., MATSUWAKI, U., OTSUKA, Y., KATAGIRI, G., KATO, M., MATSUBARA, K., AOYAMA,Y.&JINNAI, H. (2010). Direct three- dimensional visualization and morphological analysis of Pt particles supported on carbon by transmission electron microtomography. In Handbook of Fuel Cells – Fundamentals, Technology and Applications, pp. 1–8. Chichester: John Wiley & Sons, Ltd.
JARAUSCH, K.F. & LEONARD, D.N. (2007). Enabling 360 degree TEM/ STEM of nanoparticles. Imaging Microsc 9,24–27.
JIANG, Y.,HOVDEN, R.,MULLER, D.A. & ELSER, V. (2014). Compressed sensing, sparsity, and the reliability of tomographic reconstructions. Microsc Microanal 20, 796–797.
JINNAI, H., NISHIKAWA, Y., SPONTAK, R.J., SMITH, S.D., AGARD, D.A. & HASHIMOTO, T. (2000). Direct measurement of interfacial curvature distributions in a bicontinuous block copolymer morphology. Physical Review Letters 84, 518–521.
JINNAI, H., SPONTAK, R.J. & NISHI, T. (2010). Transmission electron microtomography and polymer nanostructures. Macromolecules 43, 1675–1688.
KAWASE, N., KATO,M.,NISHIOKA,H.&JINNAI,H. (2007). Transmission electron microtomography without the ‘missing wedge’ for quantitative structural analysis. Ultramicroscopy 107,8–15.
KE, X., BALS, S., COTT, D., HANTSCHEL, T., BENDER,H.& VAN TENDELOO, G. (2010). Three-dimensional analysis of carbon nanotube networks in interconnects by electron tomography without missing wedge artifacts. MicroscMicroanal 16,210–217.
KIZUKA, T., SUMI, T., BANSHO,S. & SAITO, T. (2001). Three- dimensional imaging of carbon nanotubes. Jpn J Appl Phys 40, L56–L58.
KROON, D.-J. (2010). Smooth triangulated mesh. MATLAB Central File Exchange. Available at
https://www.mathworks.com/ matlabcentral/fileexchange/26710-smooth-triangulated-mesh (retrieved April 30, 2017).
KROON, D.-J. (2014). Patch curvature. MATLAB Central File
Exchange. Available at
https://www.mathworks.com/matlacentral/ fileexchange/32573-patch-curvature (retrieved February 9, 2017).
LANZAVECCHIA, S., CANTELE, F., BELLON, P.L., ZAMPIGHI, L., KREMAN, M., WRIGHT,E.&ZAMPIGHI, G.A. (2005). Conical tomography of freeze-fracture replicas: A method for the study of integral membrane proteins inserted in phospholipid bilayers. J Struct Biol 149,87–98.
LEARY, R., SAGHI, Z., MIDGLEY, P.A & HOLLAND, D.J. (2013). Compressed sensing electron tomography. Ultramicroscopy 131,70–91.
LEVIN, B.D.A., PADGETT, E., CHEN, C.-C., SCOTT, M.C., XU, R., THEIS, W., JIANG, Y., YANG, Y., OPHUS, C., ZHANG, H., HA, D.-H., WANG, D., YU, Y., ABRUÑA, H.D., ROBINSON, R.D., ERCIUS, P., KOURKOUTIS,L.F., MIAO,J., MULLER,D.A.&HOVDEN, R. (2016). Nanomaterial datasets to advance tomography in scanning transmission electron microscopy. ScientificData 3, 160041.
MASTRONARDE, D.N. (1997). Dual-axis tomography: An approach with alignment methods that preserve resolution. J Struct Biol 120, 343–352.
MIDGLEY, P.A. & WEYLAND, M. (2003). 3D electron microscopy in the physical sciences: The development of Z-contrast and EFTEM tomography. Ultramicroscopy 96, 413–431.
PALMER, C.M. & LÖWE, J. (2014). A cylindrical specimen holder for electron cryo-tomography. Ultramicroscopy 137,20–29.
PREIBISCH, S., SAALFELD,S. & TOMANCAK, P. (2009). Globally optimal stitching of tiled 3D microscopic image acquisitions. Bioinformatics 25, 1463–1465.
SAGHI, Z., DIVITINI, G.,WINTER, B., LEARY, R., SPIECKER, E., DUCATI,C. &MIDGLEY, P.A. (2016). Compressed sensing electron tomography of needle-shaped biological specimens – Potential for improved reconstruction fidelity with reduced dose. Ultramicroscopy 160, 230–238.
SAGHI, Z., HOLLAND, D.J., LEARY, R., FALQUI, A., BERTONI, G., SEDERMAN, A.J., GLADDEN, L.F. & MIDGLEY, P.A. (2011). Three- dimensional morphology of iron oxide nanoparticles with reactive concave surfaces. A compressed sensing-electron tomography (CS-ET) approach. Nano Letters 11, 4666–4673.
WANG, X., SHAH, F.A., PALMQUIST,A.&GRANDFIELD, K. (2017). 3D characterization of human nano-osseointegration by on-axis electron tomography without the missing wedge. ACS Biomater Sci Eng 3,49–55.
WARD, E.P.W., YATES, T.J.V., FERNÁNDEZ, J.-J., VAUGHAN, D.E.W. & MIDGLEY, P.A. (2007). Three-dimensional nanoparticle distribution and local curvature of heterogeneous catalysts revealed by electron tomography. The Journal of Physical Chemistry C 111, 11501–11505.
WEYLAND,M. & MIDGLEY, P. (2016). Electron tomography. In Transmission Electron Microscopy, vol. 506, Carter, C. B. & Williams, D. B. (Ed.), pp. 343–376. Cham: Springer International Publishing.
APPENDIX:SPECIMEN PREPARATION PROCEDURE SUMMARY
1. Clean needles with oxygen or argon plasma. 2. Mix fibers in ethanol and Nafion binder (as needed) and ultra-sonicate untilwell dispersed. Suggested concentration: 0.5mg fibers per 1mL ethanol, 0.02 wt% Nafion solution.
Page 1 |
Page 2 |
Page 3 |
Page 4 |
Page 5 |
Page 6 |
Page 7 |
Page 8 |
Page 9 |
Page 10 |
Page 11 |
Page 12 |
Page 13 |
Page 14 |
Page 15 |
Page 16 |
Page 17 |
Page 18 |
Page 19 |
Page 20 |
Page 21 |
Page 22 |
Page 23 |
Page 24 |
Page 25 |
Page 26 |
Page 27 |
Page 28 |
Page 29 |
Page 30 |
Page 31 |
Page 32 |
Page 33 |
Page 34 |
Page 35 |
Page 36 |
Page 37 |
Page 38 |
Page 39 |
Page 40 |
Page 41 |
Page 42 |
Page 43 |
Page 44 |
Page 45 |
Page 46 |
Page 47 |
Page 48 |
Page 49 |
Page 50 |
Page 51 |
Page 52 |
Page 53 |
Page 54 |
Page 55 |
Page 56 |
Page 57 |
Page 58 |
Page 59 |
Page 60 |
Page 61 |
Page 62 |
Page 63 |
Page 64 |
Page 65 |
Page 66 |
Page 67 |
Page 68 |
Page 69 |
Page 70 |
Page 71 |
Page 72 |
Page 73 |
Page 74 |
Page 75 |
Page 76 |
Page 77 |
Page 78 |
Page 79 |
Page 80 |
Page 81 |
Page 82 |
Page 83 |
Page 84 |
Page 85 |
Page 86 |
Page 87 |
Page 88 |
Page 89 |
Page 90 |
Page 91 |
Page 92 |
Page 93 |
Page 94 |
Page 95 |
Page 96 |
Page 97 |
Page 98 |
Page 99 |
Page 100 |
Page 101 |
Page 102 |
Page 103 |
Page 104 |
Page 105 |
Page 106 |
Page 107 |
Page 108 |
Page 109 |
Page 110 |
Page 111 |
Page 112 |
Page 113 |
Page 114 |
Page 115 |
Page 116 |
Page 117 |
Page 118 |
Page 119 |
Page 120 |
Page 121 |
Page 122 |
Page 123 |
Page 124 |
Page 125 |
Page 126 |
Page 127 |
Page 128 |
Page 129 |
Page 130 |
Page 131 |
Page 132 |
Page 133 |
Page 134 |
Page 135 |
Page 136 |
Page 137 |
Page 138 |
Page 139 |
Page 140 |
Page 141 |
Page 142 |
Page 143 |
Page 144 |
Page 145 |
Page 146 |
Page 147 |
Page 148 |
Page 149 |
Page 150 |
Page 151 |
Page 152 |
Page 153 |
Page 154 |
Page 155 |
Page 156 |
Page 157 |
Page 158 |
Page 159 |
Page 160 |
Page 161 |
Page 162 |
Page 163 |
Page 164 |
Page 165 |
Page 166 |
Page 167 |
Page 168 |
Page 169 |
Page 170 |
Page 171 |
Page 172 |
Page 173 |
Page 174 |
Page 175 |
Page 176 |
Page 177 |
Page 178 |
Page 179 |
Page 180
