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Chromatography 27


New HPLC On-Line Solution Secures the Analytical Workflow of Pharmaceutical Laboratories


High Performance Liquid Chromatography (HPLC) has been and continues to be a workhorse of the pharmaceutical laboratory. Throughout the product life cycle from Pre-Formulation to Quality Control, HPLC coupled to Dissolution and Content Uniformity/Assay testing are some of the biggest sample sources for HPLC analysis.


Sotax, a leader in automated solutions for dissolution testing and automated sample prep has developed a variety of ‘Off- line’ autosampler solutions over the decades. ‘Off-line’ samples are withdrawn from their instruments, immediately filtered and collected in a variety of formats.


To further automate the analytical workflow and to avoid costly manual transfer mistakes, Sotax is now pleased to announce the newest addition to their line of autosamplers: the SAM Sample Manager.


The SAM guarantees a seamless flow from Dissolution samples to analytical results. Totally flexible and scalable, the system is available in three different capacities to connect to semi-automated dissolution systems and fully-automated dissolution systems: SAM S (small; for up to 240 samples), SAM M (medium; for up to 480 samples), and SAM L (large; for up to 720 samples). The SAM acts as a transfer platform keeping samples protected and injecting them one by one into HPLC, all without any vial transfer.


The system works with any HPLC instrument with ready signal functionality and can be integrated with a variety of different injection valves.


SAM is driven by the WinSOTAXplus Advanced Dissolution Software while the LC data is processed with the existing chromatography software. SAM will take care of the samples seamlessly from start, to analytical finish.


MORE INFO. 73 MORE INFO. 74 Release of a New Control Driver for ELSD System


DataApex is pleased to announce the release of a new control driver for the Evaporative Light-Scattering Detector 90LT, manufactured by Sedere Company. This is already the 3rd Sedere detector its control and digital data acquisition has been incorporated into Clarity Chromatography SW. The driver for ELSD 90LT has been officially released with Clarity Chromatography Software version 4.0.3. Sedere is a leading manufacturer of Low-Temperature Evaporative Light-Scattering Detectors. Sedere has more than 25 years of experience in the development of versatile detection systems for all chromatography applications and their detectors are distributed worldwide.


Clarity Chromatography Software has a strong position in the chromatography data systems market. Clarity, the third generation of DataApex products, allows controlling more than 400 different instruments from the single environment and offers its users very high flexibility. Clarity is highly regarded for its intuitive approach, excellent performance, cost-effectiveness and proficient technical support. DataApex is solely focused on chromatography software development. A strong emphasis is placed on technological innovation, visionary adoption of new laboratory standards, best practices and extensive customer support. DataApex products are sold in over 80 countries around the world. Ten chromatography instrument manufacturers privately resell labelled versions of DataApex’s software.


MORE INFO. 75


Cost-Effective Gas Chromatograph


BFRL’s SP-3420A is a cost-effective gas chromatograph, ideal for routine analysis. It accommodates standard and capillary injectors. Two ionisation detectors or one TCD may be installed. The column oven accepts packed or fused silica capillary columns. On board computer guides you through operation via the on line display and the self-diagnostic capability allows you to test instrument condition and to detect and identify faulty circuits. In addition, continuous testing is done by the instrument to detect possible electronic failures. Many detectors are available, such as TCD, FID, ECD, FPD and TSD. Also wide selections of injectors are available with the most common being split/splitless, packed and on-column.


The Company offers eight series of over 50 models of products, including atomic absorption spectrophotometer, atomic fluorescence spectrometer, FTIR spectrometer, UV/VIS spectrophotometer, optical emission spectrometer, gas chromatography, high performance liquid chromatography and microwave digestion system, all offered at very competitive prices.


MORE INFO. 76


HPLC Columns Now Available With 3 Micron Particles


Thermo Fisher Scientific is pleased to announce that Thermo Scientific™ Syncronis™ HPLC columns are now available with 3mm. particle size. This new particle size complements the existing 1.7 and 5µm particle sizes.


“This builds on the heritage of the Syncronis family of LC columns, which offer consistent, reproducible separations with high loadability,” said Darren Thomas, Thermo Fisher Scientific General Manager, Chromatography Consumables.”This is an excellent solution for those scientists that have standardised their separations on 3mm particle size.The expanded range of Syncronis columns matches a diversity of requirements from fast method development to rugged QC and high efficiency preparative LC.”


Syncronis columns are built on a backbone of highly pure, high surface area silica. Dense bonding and double endcapping minimise variation due to silanol activity. Enhanced automated column packing methods drive consistency even further, and each column is individually tested.


MORE INFO. 77 MORE INFO. 78


Beijing Beifen-Ruili Analytical Instrument (Group) Co. Ltd.


Tel: 0086 10 84347289, 64361325 Fax: 0086 10 64377039


Email: international@bfrl.com.cn or market@braic.com


Website: www.bfrl.com.cn or www.braic.com


INTERNATIONAL LABMATE - JANUARY/FEBRUARY 2013


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