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Reactor-ReadyTM
Pilot Lab Reactor
The new Reactor-Ready Pilot from Radleys is a universal pilot scale jacketed reaction system which has been designed for use with a range of vessels from 5 to 20 litres. Developed following the incredible success of the smaller bench-top Reactor-Ready lab reactor (100ml to 5 litres), the Pilot system offers many labour saving features not normally available in larger scale systems like this.
The beauty of Reactor-Ready Pilot is that this one reactor workstation can replace multiple frameworks, saving fume hood space and costs on multiple set-ups. A range of interchangeable process vessels (1.25 to 1 ratio, which mimic plant scale reactors) makes Pilot ideal for process development, scale-up, pilot and kilo labs. The patented vessel collar and clamp design allows different vessel sizes to be loaded into the single framework, the lid attached and stirrer aligned in just minutes. All vessels operate across a temperature range of -70°C to +230°C.
Other features include quick-release clamp and hose couplings which allow rapid vessel change-over, without the need for tools. Wide bore hose and vessel connections offer maximum flow rates and heating/cooling performance, with innovative hose manifolds for easy thermofluid drain down during vessel exchange. Additionally, a novel self-aligning stirrer coupling allows the overhead stirrer to engage with the stirrer for powerful stirring up to 800rpm.
Reactor-Ready Pilot is supplied with castor as standard but feet are also included, allowing the system to be in a fixed position or mobile. The adjustable stainless steel framework incorporates a spirit-level for fine levelling and a range of clamps, accessory glassware, baffles and drip trays which mean Reactor-Ready Pilot can be customised to meet the needs of almost any process laboratory.
For further information on Reactor-Ready Pilot please contact Radleys or visit the website.
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Overhead Stirrer Provides an Effective Tool for Rapid Screening
An independent report (
www.asynt.com/download_files/84.pdf) demonstrates how the Asynt Vortex overhead stirrer system provides an effective tool for rapid screening of a range of reaction conditions in parallel - an essential for efficient process development.
The Asynt Vortex overhead stirrer system is designed to enable three reactions to be stirred simultaneously using a single overhead stirrer motor and heated to temperatures to over 200°C.
In the report - researchers evaluate the consistency of mixing delivered by a Vortex system controlling three reaction vessels by measuring the bulk mixing and extraction times in each vessel and comparing this data with a stand-alone vessel.
From the experiments conducted - the researchers concluded that no significant difference was measured in the mixing capability of a reaction vessel connected to a Vortex system when compared to a stand-alone single reaction vessel set-up. In addition the mixing characteristics across the three reaction vessels set up on the Vortex system were, within experimental error, the same. Therefore the researchers concluded that the Vortex system constitutes a useful addition for laboratories conducting parallel synthesis minimising both the necessary laboratory footprint required and reducing the cost significantly by replacing three overhead stirrers with one. Further the integration of the Vortex with an Asynt DrySyn Multi hotplate allows heating of the three reaction vessels using a single hotplate also reducing the space requirements and costs when compared to a standard set-up without the mess and safety concerns of using a conventional oil bath system.
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21.01.14 11:42
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