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Direct Adaptive HPLC Column Connectors


When changing from a Waters column to another brand like an Agilent Column, do you find changing the ferrules and tubing (to maintain data integrity) time consuming? If so, Microsolv Technology Corporation have a solution that can help, introducing the MicroSolv™ Direct Adaptive (Di-Ad™) HPLC Column Connecters. They make this process much faster and easier without fussing with ferrules and tubing between column changes.


These Direct Adaptive Fittings were designed for you to avoid poor column connections and eliminate extra system volume. The universal pilot length of this spring-loaded connector adapts to any HPLC column for quick column swaps and prevention of poor connections that cause peak broadening. Available as a Single End Fitting or a Double End Fitting. You just simply screw the Di-Ad™ fittings into the column and the tubing pilot length will automatically be adjusted.


More information online: ilmt.co/PL/Ey50 Ready for the Future of Rapid Trace PFAS Screening


The analysis of polyfluoroalkyl substances (PFAS) is a well-discussed topic in today’s environmental market. Due to concerns about the effect on human health and environmental risks, measurements of PFAS concentrations in a wide variety of matrices are conducted. These studies aim to get a better insight into the effects of PFAS substances.


To underline the importance of this subject, a proposal to restrict the use of per- and polyfluoroalkyl substances (PFAS) was submitted in January 2023 to the ECHA by several European countries. This proposal aims to ultimately ban the use of PFAS substances.


Traditional PFAS analytical methods are focused on the speciation of the individual PFAS components with expensive separation techniques. Currently, thousands of PFAS components have been produced and identified for monitoring, which makes the analyses for these components more and more complex.


Due to this, there is a growing request for a standardised, fast and reliable PFAS screening method to optimise the sample throughput and reduce resources. TE Instruments’ solution for PFAS screening is the Xprep C-IC, designed to determine the total amount of PFAS components in aqueous matrices at ultra-low trace levels.


The determination of AOF (Adsorbable Organic Fluorines) is based on the same principle as AOX (Adsorbable Organic Halogens) analyses: A generally accepted and standardised technique used for decades in environmental laboratories for the monitoring of the levels of organic halides (Chlorine/ Bromine/Iodine) in aqueous matrices. Where a sample is combusted, conditioned, and quantified by means of coulometric titration. For the analyses of AOF, the quantification step is performed by the use of an Ion Chromatograph (IC).


TE Instruments developed a fully automated, extremely compact sample preparation system covering oxidative pyrohydrolytic combustion, fraction collection, and sample injection towards the IC. The Xprep C-IC can introduce samples both via optimised direct injection (liquids module) and conventional boat-inlet (boat module) into a horizontal furnace. This automated sample-prep solution reduces the complexity of sample transfer and significantly improves user convenience.


A unique feature of the Xprep C-IC setup is the optional usage of a ceramic insert in the furnace combustion tube. While standard AOX analysis focuses on standard halides, the analysis of PFAS is mainly aimed at the analysis of elemental Fluoride. This is where the power of the ceramic insert comes into its place. In a standard situation, Fluoride attacks quartz glass and may thus create a defective combustion tube over time. With the usage of the ceramic insert, a protective layer protects the furnace tube quartz material resulting in a far longer lifetime compared to a standard quartz glass setup.


Are you interested in the analytical solutions TE Instruments has to offer? Please feel free to contact us for more information or challenge us with your application request.


More information online: ilmt.co/PL/5qbm Rapid Scanning UV Detector with High-Temperature Flow Cell


Testa Analytical Solutions eK has added a high-temperature flow cell to its rapid scanning UV Detector, expanding its capabilities. The durable flow cell utilises fibre optic connections to connect the rapid scanning UV detector, allowing it to be safely located up to one meter away from the high-temperature process under observation.


This high-performance UV monitor was initially designed to function within the heated sample compartment of a Gel Permeation Chromatography (GPC/SEC) system, enabling operation at temperatures as high as 210°C.


The remote flow cell is offered in various configurations, catering to UV monitoring needs of analytical to preparative scale processes. This innovative device facilitates highly precise UV measurements on high-temperature process samples that would otherwise be challenging to make through direct spectroscopic measurements.


More information online: ilmt.co/PL/q151 59920pr@reply-direct.com 59680pr@reply-direct.com 57858pr@reply-direct.com


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