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8 Four New Products for Enhanced Pyrolysis Analysis


Frontier Laboratories Ltd has launched four new products around the Multishot Pyrolyzer EGA/PY-3030D, their state-of-the-art vertical furnace pyrolyser (for Py-GC/MS), equipped with a programmable ceramic heater, enabling, beside single shot pyrolysis, thermal desorption, heart cut and evolved gas analysis.


The Micro-Jet Cryo-Trap MJT-2030E is an excellent tool for energy effi cient rapid cooling and instant thermal desorption (TD-GC/MS). Trapping of low boiling compounds (CO2


analysis of gases evolved from Multishot Pyrolyzer. The Selective Sampler SS-2010E is provides Heart-Cutting of desired Peaks and comes with a new Flow Switching System.


Various atmosphere gases (He, Air, etc) can be used. The Multi-Functional Sampler MFS-2015E makes splitless Pyrolysis possible without compromises, enabling 100x improved sensitivity (with LOQs in pg range). The MFS shortens analysis time by backfl ushing, solvent venting is also possible. It is the ideal tool for trace analysis, such as µ- and nano-Plastics, and additives detection. The new Cryogenic Mill IQ MILL-2070 is easy to use and simple to operate. Fast and effi cient high-speed milling is enabled by 3D/8-fi gure crushing ball motion. It pulverises samples at highest uniformity, homogeneity, and reproducibility.


More information online: ilmt.co/PL/QB5n 57135pr@reply-direct.com , ethane, etc) is possible due to the liquid nitrogen jet fl ow and cooling temperature of -196ºC. It enables automatic heart cut


Quality Control and Optimisation of Coating Processes using Ion Chromatography


Surface fi nishing such as electroplating is one of the most important industrial processes to design products with dedicated physical, chemical, and electronic properties. Purity and composition of solutes, solvents, catalysts, and the electrolytic baths are a key requirement to achieve the desired properties, prevent damages and inferiority of the products by imbalances or contaminations. Impurities, even on an ultratrace level, can have detrimental effects for example on the electrical properties of integrated circuits and fi nal products in the semiconductor industry. Therefore, Semiconductor Equipment and Materials International (SEMI) stipulates for many basic chemicals and raw materials impurity levels in the low µg/L range. Ion chromatography (IC) is the ideal method for analysing ionic impurities, even in the ng/L range.


Impurities like fl uoride, chloride, bromide, nitrite, nitrate, phosphate, or sulphate may alter the properties of a bath. Consequently, the plating properties are impaired or the semiconductor even damaged. Chemicals and raw materials used for process solutions, such as etching, plating, or cleaning solutions, need to be virtually free of such ionic impurities. IC, combined with Inline Matrix Elimination and Inline Preconcentration, is ideal to determine such impurities even in ultratraces.


Inline Matrix Elimination removes uncharged or oppositely charged matrix components (e.g., hydrogen peroxide), thus reducing sample preparation and improving the column lifetime. Additional combination with the intelligent Inline Preconcentration increases the measuring sensitivity, allowing the analysis of impurities in the ng/L range.


Example applications include: Trace anion and cation analysis in ultrapure water, Trace anion analysis in acids, Chloride and sulphate in tetramethylammonium hydroxide (TMAH) and Anionic impurities in hydrogen peroxide or organic solvents such as isopropanol.


The robustness of the of Metrohm’s technique allows to handle almost all process solutions, such as etching, extracting, or rinsing solutions. More information online: ilmt.co/PL/1pK9


57129pr@reply-direct.com


PFAS Testing Caps and Vials RSA™ Autosampler Vials for better chromatography data. Not All Vials Are Created Equal


An Electronic Leak Detector is indisipensable for finding small leaks around fittings or hot inlets. Leaks present can give cause to baseline instability. The LD239 is an easy way to quickly identify leaks in your system.


• Compact Handheld Device (50x20x111mm)


Only RSA™ l Prevent pH Changes


l Great for Bio-Active


Compounds Prevent hydrolysis in your vial due to glass with reduced surface silanols.


l Minimize Sample


Adsorption Insure quantitation precision run to run for low abundance basic compounds.


EXCLUSIVELY BY: TRY THEM TODAY! www.rsa-glass.com Vials: l Prevent Adducts Seen


in the Vial Beware of ordinary borosilicate glass vials, they have variable surface chemistries.


in LCMS from the Vials Minimal surface metals.


l Cleanest Vials on the


Market Prevent spurious peaks from ordinary glass vials that contain residual manufacturing agents.


l Made with Superior


Dimensional Control Protect your sample needle and instruments.


• Highly Sensitive (0.0005 ml/min)


• USB Port Rechargeable


MicroSolv Technology Corporation™ has launched an exceptional collection of autosampler vials and caps designed for PFAS testing.


For accuracy in LCMS/MS or GCMS analysis of these compounds, the sample vials and caps used should not contain any PFAS which includes PTFE.


MicroSolv™ Polypropylene Caps and Vials are manufactured from the purest silicone rubber and pure, virgin, medical grade polypropylene, instead of traditional PTFE making them excellent for this type of analyses and will instil confi dence in laboratories who are testing for PFAS.


The vials are available in 2mL, 300ul and 700ul formats and the ultra-pure, septa cap choices are single use and closed top.


More information online: ilmt.co/PL/nZ5Y 57421pr@reply-direct.com


What’s in the next issue? Find out with a copy of our Media Information Pack.


Contact our sales team for your copy.


sales@intlabmate.com INTERNATIONAL LABMATE - APRIL 2022


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