This page contains a Flash digital edition of a book.
16 ANALYTICAL AND LABORATORY EQUIPMENT


One step filtering


The glass filter dryer is changing the filtration and drying process in laboratories worldwide. Amanda Pitcher reports.


S


ince the 19th century chemists have used the commonly known method


of Buchner filtration which would then be followed by the use of a tray dryer or other method to complete the drying phase. In 2010, glass filter dryer (GFD) technology was launched combining filtration, cake washing and drying all in one step. Working as a miniature agitated nustche filter dryer this technology allows laboratory development simulating the manufacturing process at a small scale.


Te filtration area of the smallest size ‘Mini Lab’ GFD covers 0.002m² for a total volume of 0.3L and can filter a cake volume up to 0.1L; this is a suitable piece of equipment for lab scale trials. Ten the’ Lab’ GFD size includes a removable filtration basket of 0.01m² for a cake volume around 0.5L for small scale synthesis, when the ‘Maxi Lab’ GFD is used within Kilo-Laboratory for a cake volume of 5L with 0.05m² filtration area.


Te slurry enters the vessel through one of the nozzles located on the


vessel lid. During the filtration phase, vacuum is pulled at the bottom of the vessel while the unique filter basket collects the product. It is then possible to wash the cake, again using a nozzle of choice on the lid to introduce the solvent and the heated vessel jacket if required.


Te glass vessel is of borosilicate 3.3 construction and is pressure rated to 0.5barg. It is common practice to apply pressure to the top of the filter cake during filtration whilst the bi-directional motor is running in a clockwise direction to smooth the cake. Optimal filtration is achieved in this way as you can pressure filter with no cracks in the cake.


Te heated jacket is then used to heat the vessel for the drying phase. Te vessel is rated to temperatures between -25°C and 150°C, and it is not uncommon for the GFD to be also used for the filtration of unstable products at low temperatures. Te bi-directional motor is lowered into the cake during this phase and is now used in the anti-clockwise direction to dig into the cake thus resulting


Fig 1. Lab and Maxi Lab Glass Filter Dryer (GFD).


in the homogeneous drying of the product.


Te filtration and drying times for calcium carbonate in water in a Maxi Lab GFD are highlighted in graph 1. Tests were performed under a 0.5barg pressure for 30min to assist filtration of the solvent (deionised water) layer in 3kg of calcium carbonate. Ten loss on drying was performed on a wet cake sample.


Vacuum at -0.8barg and heating at 75°C was applied to the Maxi Lab GFD for eight hours with insulation jacket fitted to the vessel.


For more information ✔ at www.scientistlive.com/eurolab Amanda Pitcher is Product Manager,


Powder Systems Ltd (PSL), Liverpool, UK. www.powdersystems.com


Fig 2. Drying Curve of a Maxi Lab GFD. www.scientistlive.com


Page 1  |  Page 2  |  Page 3  |  Page 4  |  Page 5  |  Page 6  |  Page 7  |  Page 8  |  Page 9  |  Page 10  |  Page 11  |  Page 12  |  Page 13  |  Page 14  |  Page 15  |  Page 16  |  Page 17  |  Page 18  |  Page 19  |  Page 20  |  Page 21  |  Page 22  |  Page 23  |  Page 24  |  Page 25  |  Page 26  |  Page 27  |  Page 28  |  Page 29  |  Page 30  |  Page 31  |  Page 32  |  Page 33  |  Page 34  |  Page 35  |  Page 36  |  Page 37  |  Page 38  |  Page 39  |  Page 40  |  Page 41  |  Page 42  |  Page 43  |  Page 44  |  Page 45  |  Page 46  |  Page 47  |  Page 48  |  Page 49  |  Page 50  |  Page 51  |  Page 52