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Lube-Tech PUBLISHED BY LUBE: THE EUROPEAN LUBRICANTS INDUSTRY MAGAZINE


One DLC is described as 50%sp3 second DLC is described as sp2


; 40% hydrogen content; the ;Cr doped; 0% hydrogen. Both


types of DLC ball were provided by PCS Instruments.


No.110 page 3


Figure 7. Grey-scale and computer enhanced wear images


Figure 8 shows an example of how the wear scar of the disc is estimated. Unlike the ball, it is not possible to measure the wear across the whole circumference of the disc therefore only a small cross-section of the disc is examined. This type of measurement was taken at 8 different points around the wear track and an average value calculated. Whilst we do not measure the whole wear track, the measurement allows quantitative comparisons between oils to be measured.


Table 1. Steel ball and DLC ball profiles used in MTM sliding contact


The effect of friction modifiers in a steel ball – steel disc contact was also investigated and compared to DLC ball – steel disc arrangement.


Friction and Wear tests were conducted using a PCS Instruments Mini Traction Machine, using the following test profile: • Determination of an initial Stribeck curve: • Ball on disc: Pure Sliding • Virgin surfaces • Load 36N (1.01 GPa Hertzian Pressure) • Lubricant temperature 80ºC • Entrainment speeds between 0.05 m/s and 3.0 m/s • No running-in profile, friction measured from high speed to low speed


• Run a rubbing test profile; pure sliding, 0.05 m/s at 30 N and 80ºC for 120 mins


• Determination of a Second Stribeck curve using the same conditions described above for the initial Stribeck curve. Friction and wear performance was determined after the second Stribeck curve was generated.


Following completion of the second Stribeck curve, wear profiles for both balls and discs were studied using 3D imaging (Bruker 3D Optical Profilometer Contour GT).


Figure 7 shows examples of both grey scale images and computer enhanced images of the wear scar observed on the ball. Using these images the volume of the wear scar can be estimated.


Figure 8. Example of wear determination of the steel disc


2.1 Test Samples The 5W30 European ACEA C3 oil was once again used as the base line reference fluid. Friction modifiers were added to this reference oil in order to determine the influence of MoDTC, polymeric friction modifiers and a conventional organic friction modifier, namely glycerol mono-oleate (GMO).


The test samples and tests conducted are shown in Table 2.


Table 2. Samples and tests conducted using MTM sliding conditions LUBE MAGAZINE NO.139 JUNE 2017 35


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