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Mass Spectrometry & Spectroscopy 27


New XRD System Announced at JASIS 2017


At the Japan Analytical Scientific Instruments Show (JASIS), Bruker announces the new D8 DISCOVER PlusTM X-ray diffraction (XRD) system. The D8 DISCOVER Plus combines the high power of the new TXS-HETM high- efficiency Turbo X-ray SourceTM with the unrivalled reliability and accuracy of the new high endurance ATLASTM goniometer.


The TXS-HE is optimised to deliver an extremely high intensity X-ray beam without compromising flexibility to meet the most demanding analytical needs in today’s research, development and process control. The TXS- HE significantly reduces data collection time compared to conventional X-ray sources and delivers better data quality, giving new insights into structural properties of investigated materials. Further, the additional speed of the TXS-HE enables the studies of dynamic processes including time dependent phase transitions and kinetics in materials better than ever before.


The advanced design of the new ATLAS goniometer delivers an even higher level of angular positioning accuracy, thus increasing the reliability of measured data for all applications. It is extremely robust ensuring that this level of performance is maintained for all configurations from classic powder diffraction to epitaxial thin-film characterisation. As a result, the D8 DISCOVER Plus with ATLAS goniometer even tops Bruker’s unique total system alignment guarantee, setting the new standard for XRD laboratory systems.


By combining the high X-ray flux of the TXS-HE, the outstanding accuracy of the ATLAS goniometer, and the large detection area and dynamic range of the new EIGER2 R 500K multi-mode Hybrid Photon Counting (HPC) detector, the D8 DISCOVER Plus offers unmatched capabilities for the analytical tasks in materials research and analysis.


“With the introduction of the D8 DISCOVER Plus, Bruker once again sets new standards in XRD instrumentation. The D8 DISCOVER Plus is designed to deliver top-class results for structure analysis of all kinds of materials, from powders in the pharmaceutical industry to crystalline structures in semiconductor devices, and is a further step to strengthen Bruker’s position as the provider of the most powerful and user-friendly XRD solutions on the market,” stated Dr Lutz Bruegemann, General Manager XRD and Vice President of Bruker AXS.


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New Single Quadrupole Mass Spectrometer and Specialised Columns Designed to Deliver Reproducible and Robust Separations, Increase Analytical Accuracy


Thermo Fisher Scientific Inc has announced new technologies that are designed to allow analytical chemists to obtain high-resolution separations with outstanding sensitivity and reproducibility.


“Our customers want gain a deeper understanding of their samples,” said Mitch Kennedy, Vice President and General Manager, Life Sciences Business, Chromatography and Mass Spectrometry, Thermo Fisher. “At HPLC, we demonstrated to customers our commitment to innovation and to equipping them with the necessary tools to make their journey from sample to knowledge easier so they can solve their most complex analytical challenges.”


The new Thermo Scientific ISQ EC Single Quadrupole mass spectrometer seamlessly integrates with an existing ion chromatography (IC) or high performance liquid chromatography (HPLC) system and provides excellent small molecule sensitivity and mass confirmation for users. The industry-leading Chromeleon Chromatography Data Software (CDS) platform has embedded ISQ EC MS instrument control, which enables users to minimise time spent on new mass spectrometry (MS) user training. The instrument also provides exceptional robustness, enabling users to analyse a range of simple and complex sample matrices.


The new range of Thermo Scientific MAbPac RP 1mm columns, which are designed to provide the resolution and ruggedness required for high-performance, reversed-phase chromatography characterisation of monoclonal antibodies, fragments, variants, antibody drug conjugates and proteins. With a 1mm inner diameter, the new columns provide sensitive analyses of very small sample volumes at low flow rates for direct injection into the LC-MS, thus streamlining workflows and achieving high sensitivity. Featuring a polymeric resin with an optimised pore size and thermal and pH stability, the new columns allow consistent and efficient separations with low carry-over.


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