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Environmental Analysis & Electrochemistry


10. Henderson A, Heaney LM, Rankin-Turne S. Ambient ionisation mass spectrometry for drug and toxin analysis: A review of the recent literature. Drug Test Anal. 2024;16:1323–44. doi: 10.1002/dta.3644.


11. Bueno C, Harrison A, Ruiz G, Martínez L, Stahl-Zeng J. Quantitation of mycotoxins and tropane alkaloids in food using SCIEX 7500+ system and QTRAP technology. SCIEX Technical Note. Available at: https://sciex. com/tech-notes/food-beverage/food-and-beverage/Quantitation-of-mycotoxins-and-tropane-alkaloids-in- food-using-SCIEX-7500--system-and-QTRAP-technology. Accessed March 17, 2025.


12. Martinez L, He L. Detection of Mycotoxins in Food Using Surface-Enhanced Raman Spectroscopy: A Review. ACS Appl Bio Mater. 2021;4:295–310. doi: 10.1021/acsabm.0c01349.


13. Jafari S, Guercetti J, Geballa-Koukoula A, et al. ASSURED Point-of-Need Food Safety Screening: A Critical Assessment of Portable Food Analyzers. Foods. 2021;10:1399. doi: 10.3390/foods10061399.


14. SCIEX 7500+ System. Setting a new standard for instrument resilience. Available at: https://sciex.com/ products/mass-spectrometers/triple-quad-systems/triple-quad-7500-plus-system. Accessed March 1, 2025.


15. The SCIEX 7500+ system launches at ASMS 2024. SCIEX Press Release. June 3, 2024. Available at: https://sciex.com/about-us/press-releases/2024/sciex-7500plus-system-launches-at-asms2024. Accessed March 1, 2025.


16. Lee H, Moore I, Butt CM, Jones E. Achieving exceptional robustness for PFAS analysis in food with the next-generation SCIEX 7500+ system. SCIEX Technical Note. Available at: https://sciex.com/tech-notes/ food-beverage/food-and-beverage/achieving-exceptional-robustness-for-pfas-analysis-in-food-with-the-next- generation-sciex-7500-plus-system. Accessed March 11, 2025.


17. Stahl-Zeng J, El Khallabi H, Steed J, Bueno C, Moore I. Ultra-fast MRM acquisition and quantitation of food contaminants in multiple food matrices. SCIEX Technical Note. Available at: https://sciex.com/ content/dam/SCIEX/pdf/tech-notes/food-and-beverage/food-and-beverage/MKT-31501-A_Pesticides- mycotoxins-7500%20plus_Final..pdf. Accessed March 11, 2025.


18. QTRAP Technology. SCIEX Application Note. Available at: https://theanalyticalscientist.com/fi leadmin/ tas/issues/App_Notes/00717-app-note-sciex-supplied.pdf. Accessed March 1, 2025.


Read, Share and Comment on this Article, visit: www.labmate-online.com


The preparation of environmental samples in environmental chemistry


Routine digestion and leaching of environmental samples, like soil, sediments, sludge, fly ash, etc., are among the most-used applications in environmental chemistry for the preparation of samples for element analysis.


Anton Paar’s Multiwave systems adhere to the most stringent requirements, including those published by the US Environmental Protection Agency (EPA), which provides an official compendium of approved analytical and sampling methods. The accuracy of these methods depends on precise replication of the defined reaction conditions (chemistry and temperature profiles). Anton Paar offers a broad range of instruments that fit the specific requirements of our customers.


Anton Paar’s rotor-based instruments, Multiwave 5000 and Multiwave GO Plus, feature an innovative SmartVent vessel technology that sets an industry benchmark of precision. This venting technology in our HVT vessels is used to effectively release reaction gases at controlled pressures, enhancing the robustness of the sample preparation method. The design ensures consistent and reliable results, even with complex environmental samples, which is essential for laboratories requiring efficient and accurate analysis of environmental samples.


Multiwave 5000 and Multiwave GO Plus provide preinstalled generic methods that simplify the work needed for method development. Routine testing methods like EPA 3015A, EPA 3051A or EPA 3052 are preinstalled and simplify the overall workflow in laboratories. The Multiwave instruments facilitate fast methods for higher sample amounts (1 g to 3 g) too.


Multiwave 5000 and Multiwave GO Plus provide a comprehensive methods library, including EPA methods, that is already installed (e.g. EPA 3015A, 3051A, 3052). Precise IR-temperature measurements on all vessel positions show any vessel-to-vessel deviation in temperature. Multiwave 5000 also provides full documentation of each single sample for GLP compliance.


According to the needs of environmental laboratories, a comprehensive range of different rotor types allows users to adjust to the required throughput and quantity of samples. Depending on the configuration selected, customers can maximise their throughput with rotors of up to 41 samples, or optimise the sample quantity with vessels of up to 100 ml total volume.


Mercury and arsenic are difficult elements to be routinely determined in different samples (e.g. fly ashes) because of the potential losses of volatile elements. Reliable leaching for mercury, arsenic and other environmentally-relevant elements can be achieved with the pressure-activated venting vessels of the different HVT rotors of Multiwave GO Plus and Multiwave 5000. The same quality results can also be achieved using a hermetically sealed high-pressure vessel, resulting in complete recoveries of volatile elements like mercury and arsenic and all studied elements like Cd, Cu, Ni, Pb, and Zn.


More information online: ilmt.co/PL/xw05 62802pr@reply-direct.com Advanced spectrophotometry for water quality and analytical applications


The Lovibond® XD 7500 (UV-VIS) spectrophotometer is a versatile tool for water quality monitoring and a range of other analytical applications. Equipped with a premium optical system and reference beam technology, it ensures high precision and reliability. Automatic test recognition, facilitated by an internal barcode reader, streamlines the testing process, while features such as automatic cuvette detection and over 170 pre-programmed methods simplify the workflow.


Both the XD 7000 and XD 7500 models are designed to meet a wide range of testing requirements, from routine analysis to more complex spectral scans and kinetics studies. They also support analytical quality assurance, ensuring the accuracy of the entire testing system, including the chemical methodology. Built-in security features, such as password protection and the ability to assign different levels of user rights, further enhance their suitability for use in regulated environments.


The instruments cater to various applications, including potable and wastewater analysis, process water monitoring, and R&D, where advanced features like spectral scanning and user-defined methods are useful. Data management is made easy with Ethernet, USB, and barcode scanner interfaces, ensuring seamless integration with laboratory information management systems (LIMS).


In addition, the XD series promotes cost-efficiency with low running costs, making them practical for frequent use. With their user-friendly design and multilingual support, these spectrophotometers are well-suited for global use across different industries.


More information online: ilmt.co/PL/ZR1z 63396pr@reply-direct.com


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