Industrial Chemical Applications Alcohols


Column: DB-624 125-1334 30 m x 0.53 mm, 3.00 µm


Carrier: Helium at 30 cm/sec, measured at 40°C


Injection: Split, 250°C Split ratio 1:10


Oven: 40°C for 5 min 40-260°C at 10°C/min 260°C for 3 min


Detector: FID, 300°C Nitrogen makeup gas at 30 mL/min


Sample: 1 µL of 0.01-0.05% each solvent in CS2 3,CS2 7,8 1 18, 20 26, 27 28 16 2 4 5 6


10 9


1113 12 14 15 17 21


1924 25 23


31 32 3536 34 38 33 40 45 47 46 48 51


1. Methanol 2. Ethanol 3. Isopropanol 4. tert-Butanol 5. 2-Propen-1-ol (allyl alcohol) 6. 1-Propanol 7. 2-Propyn-1-ol (propargyl alcohol) 8. sec-Butanol 9. 2-Methyl-3-buten-2-ol 10. Isobutanol 11. 2-Methoxyethanol (methyl Cellosolve) 12. 3-Buten-1-ol 13. 2-Methyl-2-butanol (tert-amyl alcohol) 14. 1-Butanol


22, 29, 30 37, 39 41, 42, 43 44 49, 50, 52 0 5 10 Time (min) 15 20 GCIC001 Suggested Supplies


Septum: Advanced Green, 5183-4759 Liner: Split, single taper, low pressure drop, glass wool, 5183-4647 Seal: Gold plated seal, 18740-20885 Syringe: 5 µL tapered, FN 23-26s/42/HP, 5181-1273


15. 2-Buten-1-ol (crotyl alcohol) 16. Ethylene glycol 17. 1-Penten-3-ol 18. 2-Pentanol 19. Glycidol 20. 3-Pentanol 21. 2-Ethoxyethanol (Cellosolve) 22. Propylene glycol 23. 3-Methyl-1-butanol (isoamyl alcohol) 24. 2-Methyl-1-butanol (active amyl alcohol) 25. 4-Methyl-2-pentanol 26. 1-Pentanol 27. 2-Penten-1-ol 28. 3-Methyl-2-buten-1-ol 29. Cyclopentanol 30. 3-Hexanol 31. 2-Hexanol 32. 4-Hydroxy-4-methyl-2-pentanone 33. Furfuyl alcohol 34. cis-3-Hexen-1-ol 35. 1-Hexanol 36. cis-2-Hexen-1-ol 37. Cyclohexanol 38. 3-Heptanol 39. 2-Heptanol 40. 2-Butoxyethanol (butyl Cellosolve) 41. cis-4-Hepten-1-ol 42. trans-2-Hepten-1-ol 43. 1-Heptanol 44. Benzyl alcohol 45. 2-Ethyl-1-hexanol 46. a-Methylphenyl alcohol 47. 1-Octanol 48. 1-Nonanol 49. 2-Phenoxyethanol 50. a-Ethylphenethyl alcohol 51. b-Ethylphenethyl alcohol 52. 1-Decanol


Agilent's new patent-pending gold inlet seal improves column lifetime by eliminating traces of machining grooves that can be the source of minute leaks.


Order online at www.agilent.com/chem/store


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