Surrogate matrix: opportunities & challenges for tissue sample analysis Review
References Papers of special note have been highlighted as: • of interest; •• of considerable interest
1
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• Compares and discusses the advantages and disadvantages of surrogate matrix approach and surrogate analyte approach. It also highlights important aspects of the validation of chromatographic methods for endogenous analytes.
3 Gilibili RR, Kandaswamy M, Sharma K, Giri S, Rajagopal S, Mullangi R. Development and validation of a highly sensitive LC–MS/MS method for simultaneous quantitation of acetyl-CoA and malonyl-CoA in animal tissues. Biomed. Chromatogr. 25, 1352–1359 (2011).
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8
Liang X, Yang L, Qin AR et al. Measuring NAD+ levels in mouse blood and tissue samples via a surrogate matrix approach using LC–MS/MS. Bioanalysis 6(11), 1445–1457 (2014).
9
Liang X, Yang L, Qin AR et al. Erratum: measuring NAD+ levels in mouse blood and tissue samples via a surrogate matrix approach using LC–MS/MS (Bioanalysis [2014] 6[11], 1445–1457). Bioanalysis 6(13), 1870 (2014).
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12 Szerkus O, Wolska E, Struck-Lewicka W et al. Development and validation of UHPLC method for the determination of cyclosporine A in biological samples. Biomed. Chromatogr. 28(6), 802–809 (2014).
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• Discusses the stability evalaution of instable compounds, which include the evalaution of bench-top and freeze–thaw stability of solid tissue.
14 Aghazadeh-Habashi A, Asghar W, Jamali F. Simultaneous determination of selected eicosanoids by reversed-phase HPLC method using fluorescence detection and application to rat and human plasma, and rat heart and kidney samples. J. Pharm. Biomed. Anal. 110, 12–19 (2015).
15 Ahonen L, Maire FBR, Savolainen M et al. Analysis of oxysterols and vitamin D metabolites in mouse brain and cell line samples by ultra-high-performance liquid chromatography-atmospheric pressure photoionization–mass spectrometry. J. Chromatogr. A 1364, 214–222 (2014).
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21 Ji QC, Zhang J, Rodila R, Watson P, El-Shourbagy T. Method development for the quantitation of ABT-578 in rabbit artery tissue by 96-well liquid-liquid extraction and liquid chromatography/tandem mass spectrometric detection. Rapid Commun. Mass Spectrom. 18(19), 2293–2298 (2004).
22 Zhang J, Todd Reimer M, Alexander NE, Ji QC, El- Shourbagy TA. Method development and validation for
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