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Soil Testing 27 Portable Water Activity Meter Helps Scientists Search for Life in Dry Valleys


Scientists from the New Zealand Terrestrial Antarctic Biocomplexity Survey (nzTABS) project are using a Decagon Devices Pawkit portable water activity meter from Labcell (UK) to study soil samples and gain a better understanding of biodiversity in the McMurdo Dry Valleys of Antarctica.


The nzTABS project, which is hosted by the International Centre for Terrestrial Antarctic Research (ICTAR) at the University of Waikato, New Zealand, is investigating biodiversity in one of the world’s coldest and driest habitats by combining soil water activity data with the results from molecular genetic and geochemical analyses. Doug McCauley and Dr Charles Lee, both of the University of Waikato, have used the Pawkit for three successive field seasons, finding it a very simple and effective way to obtain water activity (aw) measurements immediately after soil samples have been collected. The instrument’s robustness, ease of calibration and simple operation make it a straightforward task to collect reliable aw readings that are accurate to +/-0.02aw.


With extremely low water content and relative humidity, together with low temperatures, the overall conditions in the McMurdo Dry Valleys are barely sufficient


to sustain life. However, measuring water content and relative humidity are not reliable indicators of the sustainability of life, because other factors - such as the electrostatic forces around soil particles (the hygroscopic layer) and chemical bonding (hydration shells) - can trap the water, making it unavailable to organisms. On the other hand, water activity is a measure of the amount of water that is freely available, which is a far superior indicator.


Using the battery-powered, pocket -sized Pawkit is very easy: the user simply has to open the clamshell case, place the sample dish inside and press a button. Readings are obtained in just five minutes from samples of solid, liquid or powdered material, with an accuracy of +/-0.02 aw and a resolution of 0.01 aw over the instrument’s measurement range of 0 to 1.00 aw. A large, clear LCD display shows both the water activity value and the temperature at which the measurement was taken. Despite its small size, the Pawkit is a highly capable instrument thanks to the use of dielectric humidity sensor technology. The robust sensor permits operation in environmental conditions of 5-50o the calibration at any time. Battery life is typically three years.


C and 0-90% relative humidity, and it is easy to check Reader Reply Card no 96 Extraction and Evaporation – Innovative Solutions from Büchi


Innovative techniques for trace and ultra-trace analysis are one of the main challenges of chemists nowadays. Buchi offers excellent solutions for extraction and evaporation in environmental analysis: Extraction System B-811, SpeedExtractor and Syncore®


Analyst.


With the Extraction System B-811 different extraction techniques (Soxhlet Standard, Soxhlet Warm, Hot Extraction and Continuous Extraction) can be performed in one instrument without conversion of the glass assembly. Each technique follows a fully automated extraction process consisting of extraction, rinsing and drying, designed for unattended operation and minimum system handling. All instrument components in contact with solvent/sample/analyte are fully inert, which eliminates residual effects and ensures low and stable blank values.


Buchi’s new SpeedExtractor offers an even more efficient solid-liquid extraction method, using high temperature and pressure to accelerate the extraction process and to reduce the solvent consumption. With its parallel format, up to six samples can be extracted simultaneously within approximately 20 to 40 minutes.


SpeedExtractor also distinguishes itself through its high degree of user-friendliness. One advantage is that extraction cells are automatically sealed. In addition to a significant time saving, this also provides a high degree of safety as it eliminates handling errors. Furthermore, the extraction cells are preserved and its life time is extended while reproducibility is ensured. Its parallel format also significantly simplifies the programming process: the desired method is loaded, the six samples are automatically sealed, and, at the push of a button, the extraction can be started.


Flexibility is given by a temperature range of 50-200°C, a pressure range of 50-150 bar, and extraction cell sizes of 10-120 ml. The SpeedExtractor’s parallel format is ideally complemented by the parallel concentrator Syncore®


directly and therefore without any sample loss, and to be concentrated in parallel to pre-defined residual volumes. The key feature of the Syncore®


Analyst. This paired system allows for collection vessels to be transferred Analyst is an integrated


cooling zone which stores the sample in a cooled environment. The risk of cross-contamination is eliminated by an individual sample sealing system and by separated vacuum channels. Efficient and parallel concentration in less than one hour and the reduction of environmental impact due to solvent recovery makes the Syncore® of choice for concentration down to pre-defined residual volumes in trace and ultra-trace analysis.


Analyst the system Reader Reply Card no 97


Reliable Solutions for Environmental Analysis


 Büchi offers excellent solutions for extraction of soil, sludge, plastic, waste and for evaporation/concentration





 Flexibility at its best: choose from four different extraction techniques (Soxhlet, Soxhlet Warm, Hot Extraction and Continous Flow) in one system without conversion of the glass assembly  Speed: parallel pressurized liquid extraction − one batch of 6 samples ready in just 20 minutes  Reproducibility: automatic sealing of extraction cells eliminates manual, error-prone operations  No sample loss and ideal fit: direct transfer of collection vessels to Syncore®


Analyst for parallel concentration


 Time savings and high recoveries: parallel concentration to pre-defined residual volumes thanks to cooled appendix and flash back module 


BÜCHI Labortechnik AG 9230 Flawil / Switzerland T +41 71 394 63 63 www.buchi.com


Reader Reply Card no 98


Quality in your hands


November/December 2010


IET


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