A new vision for atmospheric distillation testing
Powered by innovation, the VD10 analyser from AD Systems is a new generation of laboratory analyser for automated distillation at atmospheric pressure according to ASTM D86 and similar test methods. The patented imaging system brings unmatched automation and precision to this routine analysis of fuels and solvents.
The VD10’s high-resolution digital camera visually monitors all phases of sample boiling, anticipating and predicting the optimal heater settings to respect standard method conditions for IBP, 5% timings, and distillation rate control. Just put a 100 mL sample in the flask, place it on the instrument and press START. Without any need for a pre-programming or optimisation, the instrument performs a method-compliant distillation run from the first attempt, even for unknown or difficult samples like biofuels. The user-friendly interface includes all necessary features for operation, result reporting, quality assurance and traceability, diagnostics, and LIMS communication. High-quality components, precise sensors, and robust construction assure reliability for heavy-duty, safe use with minimum maintenance. The VD10 is arguably the most advanced and innovative instrument for atmospheric distillation available today.
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tube rating for ASTM D3241 Traditionally, the amount of deposit for assessment of the thermal stability characteristics of jet fuels by ASTM D3241 was rated visually (VTR) against a reference color scale. It is recognised that human subjectivity of VTR leads to errors, and objective instrumental methods of deposit quantification was developed and became commercially available.
The automated tube rater DR10 from AD Systems was the first commercial instrument of its kind available on the market since 2011. With proven performance, the DR10 became part of ASTM D3241 ( Annex A2) and IP323 (Annex C) as the ITR technique (Interferometry Tube Rating). Since 2014 metrological methods have been declared the referee techniqueby jet fuel specification bodies (ASTM D1655, D7566, DEF STAN 91-91, JIG (AFQRJOS).
The DR10 – ITR , a stand-alone, compact instrument, can be installed in any location in minutes. Straightforward operation allows use without any training and, thanks to its rugged construction, does not require adjustments or maintenance. The operation is based on a powerful light source, a spectrometer with a fibre optic probe and specially designed application software. In less than 5 minutes the heater tube scan is completed by displaying 3D mapping of the deposit thicknesses in nanometers around the total surface of the tube. It reports maximum and average values and calculates the total volume of the deposit. With its robustness and ease of use, the DR10 is well suited for testing labs, research, refining, pipelines, terminals, and mobile laboratories—every location where the thermal oxidation stability of aviation fuel is evaluated.
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ASTM D1322 smoke point analyser In 2011, AD Systems introduced their first SP10 automated smoke point analyzer conforming to ASTM D1322 / IP598. This gave laboratories a giant leap forward from the original manual method and consequently became the referee method in jet fuel specification.
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smart analysers have been installed around the globe.
However, the technology is moving forward, and in 2020, AD Systems launched the new, improved model SP20 automated ASTM D1322 smoke point analyser. The new model has modern electronics and a redesigned user interface in 7 languages. While the SP20 strictly adheres to the test method, the level of automation has been enhanced. Thanks to its integrated ambient condition sensors, the instrument automatically records the barometric pressure at calibration and compensates for atmospheric variations when measuring. Compared to its predecessor, the new version simplifies operator work, eliminates typing errors, and improves method precision again.
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software. Beyond standard ASTM D7157 reporting of S-value, So, Sa, the SV10 calculates additional values that are widely used for oil compatibility and blending stability assessment of crude oil and marine fuels according to the CIMAC Guideline “Marine fuel handling in connection to stability and compatibility “
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The SV10 reports IN (Insolubility Number) and SBN (Solubility Blending Number) and estimates stability reserve and blending potential. The degree of asphaltenes’ insolubility (IN) and the ability of the fuel to keep asphaltenes in solution (SBN) give essential information for assessing the compatibility and blend stability of crude oils or fuels blended at different ratios.
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The ILS conducted in 2022 has demonstrated excellent repeatability and reproducibility on the SV10 analyser, twice as good as the predecessor instrument, while maintaining a good correlation with historical numbers. Besides enhanced reporting, other features like improved priming, direct access to cleaning procedures, dispensed solvents accounting, and many other small improvements make the instrument easier to use and service.
With this step forward, the SV10 is an even more valuable analytical tool capable to report aphaltenes stability, along with evaluation of fuels compatibility and blends stability.
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S-value analysis helps to assess fuels compatibility
and blend stability Significant improvements have been made to AD Systems’ SV10 Automated S-value analyser
With automation, measurement reproducibility improved fourfold. The human subjectivity and dangers posed by observing an open flame during a manual smoke point test are also a nuisance of the past. Since its launch, several hundred of these
New generation of ASTM D3241 jet fuel
thermal oxidation stability analysers AD Systems has announced the official inclusion of TO10, their innovative jet fuel thermal oxidation stability analyser, in Table 1 of ASTM D3241. The updated version D3241-24 is available from
astm.org.
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An extensive equivalency study completed in 2023 has demonstrated perfect alignment (R2 0.9914) of thermal stability results performed using the new AD Systems TO10 with those generated on the legacy equipment used to develop this test method, which are listed in Table 1.
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The new analyser was designed to raise the precision of this important test method to a new level. AD Systems carefully studied all critical test parameters, and state-of-the- art engineering solutions were implemented to develop the TO10, reducing errors while enhancing precision and reliability.
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Testing laboratories and refineries can benefit from TO10’s high precision and high throughput for their routine work certifying jet fuels in accordance with ASTM D1655, D7566, and other specifications. Lab operators enjoy a highly user-friendly instrument with low maintenance. The test sequence is fully automated from sample aeration to the rapid cooling at the end of the test. No special cleaning is required, and lab efficiency and productivity have improved drastically.
Research centres developing the next generation of Sustainable Aviation Fuels (SAF) will appreciate the TO10’s versatility. It covers a broad temperature range, and its patented dual syringe pump is ideal for analysing non-conventional samples with increased levels of viscosity or density.
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