Analytical Instrumentation


Advanced autosampler redefi nes laboratory sampling


Distillation analyser provides perfection from the fi rst drop


Atmospheric distillation is one of the most important testing methods in the process of refi ning crude oil into fuels or other petroleum products. Determining the boiling range of each distillation cut has major fi nancial implications since it allows for an increase in output from the distillation tower, and thus in the volume of fi nal products.


Anton Paar’s Diana 300 distillation analyzer - an entry-level alternative to the high-range Diana 700 that nonetheless boasts the same fuel distillation range and the same safety levels - ensures perfection from the very fi rst drop. The Diana series delivers the accuracy you need to analyze your products and maximize yield. The testing procedure and results comply with ASTM D86, ASTM D850, ASTM D1078, ISO 3405, IP 123, IP 195, JIS K 2254, and GOST 2177.


Both Diana 300 and Diana 700 cover an array of fuel samples (100 % fossil and blended fuels, like bio-fuels). Diana 700 maximizes throughput thanks to accelerated liquid-free Peltier cooling for uninterrupted measurements. They also put a premium on safety with an in-built fi re sensor and an internal fi re extinguisher that can be initiated automatically or with a button. Diana 700 and Diana 300 help refi neries get the most out of their crude oil. They can be used at tank terminals, refi neries, transportation companies and independent labs; indeed, any company that handles fuels.


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In the realm of lab automation, the critical factors of precision, effi ciency, and fl exibility stand as paramount. TE Instruments’ latest advancement, the Vectra Autosampler, is designed to simplify high-throughput sampling challenges across a spectrum of industries. This cutting-edge autosampler, equipped with innovative technology, aims to assist laboratories, whether in the (Petro) chemical, environmental, or other research sectors, into a new era of effi ciency and precision.


Operating on a revolutionary movement principle, the Vectra not only conserves bench space but also provides an expansive and fl exible working area. Featuring an integrated high-defi nition camera, it transcends its role as a basic autosampler to become a visual aid for precise position calibration. The automation of critical processes reduces the margin of operator error, while position feedback and auto-position recovery features ensure reliability and safety by adapting to unexpected changes for a seamlessly effi cient workfl ow.


With a capacity of up to 250 sample positions for standard 2 mL vials and customisable options, the Vectra is tailored to meet the dynamic demands of high-throughput labs. It incorporates high-performance conditioned trays, each with 50 positions, excelling in providing superior cooling and heating capabilities. These trays are designed to meet diverse temperature requirements, ensuring the integrity of each specimen throughout the sampling process.


The Vectra provides outstanding fl exibility in liquid handling, accommodating syringes with volumes spanning from 10 to 250 μL. This adaptability enables researchers to tailor the autosampler to diverse experimental setups, cultivating a dynamic and responsive laboratory environment. With three parking positions for syringe exchange that require no operator intervention, the Vectra guarantees uninterrupted and automated operation, reducing downtime for a smooth and effi cient lab workfl ow.


Integrating seamlessly with TE Instruments’ elemental combustion solutions, the Vectra autosampler guarantees full compliance with international test methods across diverse applications. Laboratories aspiring to elevate their capabilities and embrace cutting-edge sampling methodologies can explore the Vectra autosampler from TE Instruments. Uncover the vast possibilities and revolutionise your laboratory with this state-of-the-art solution.


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A giant leap forward for lubricity testing of aviation turbine fuels


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Paltro, the automation and A.I. division of Ducom, is excited to introduce our fully automated BOCLE 2.0 ball on cylinder lubricity tester for Aviation Turbine Fuels. BOCLE utilizes a ball on cylinder contact geometry with a steel ball loaded against a steel ring dipped in a bath containing the fuel under test. A typical test of 45 mins consist of a pre-treatment of 15 mins and actual test of 30 mins. On completion of test, the ball wear scar is measured under a microscope. The mean wear scar is an indication of the fuel lubricity with lower values associated with superior lubricity. The test parameters and test sequence is governed by ASTM D5001 standard involving a prescribed protocol.


BOCLE 2.0 automates these activities to reduce user effort and intervention thereby allowing a lab to assess fuel lubricity effortlessly for rapid decision making. Key features of BOCLE 2.0 include


• A unique hybrid automated lading, where the calibrated weight is applied automatically on completion of the pre-treatment step. A soft, motorized loading eliminates impact and jerk, completely eliminating user intervention and variability.


• A conditioned air unit with programmed logic controls the valves and the fl ow rates with automatic switch over from pre-treatment to test phase.


• Inbuilt sensors and data acquisition continuously monitor and log the test conditions for each test with a unique ID. This can be retrieved ensuring complete traceability.


• Slide-n-fi t spacers allow the lower ring to be laterally offset after a test allowing 10 tests to be conducted per ring. This allows a lab to maximize utilization of consumables.


• An intuitive and simple user interface allows user to execute the complete test sequence with a single click. Additional water level and pressure sensors alert user to routine maintenance activities. • A single source supplier for instrument, test rings, balls and accessories ensures better quality control Fully automated BOCLE 2. 0, ensures unattended operation for a 45 min test freeing up time for other activities thereby enhancing lab productivity.


Stay tuned for more news on BOCLE 2.0 automation


Paltro - building industry leading robotic test platforms and A.I enabled systems to automate sensing and improve measurements by reducing human errors and efforts. We are based in New York, USA, and pioneer in lubricants and fuel lubricity test instruments with systems such as Four Ball Tester (FBT-3), High Frequency Reciprocating Rig (HFRR 4.2) and the Fully Automated Ball-on-cylinder System (BOCLE 2.0).


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