8 New Laboratory Furniture Product Line for Mass Spectrometry and Liquid Chromatography


IonBench MS Benches are designed to ease the day to day use of your Mass Spec, by providing a signifi cant number of features that makes the use of your analytical instrument much more easier: Quieter environment with an integrated noise reduction cabinet to decrease vacuum pump noise by 75%. Cabinet can accommodates up to two vacuum pumps under the instrument and overheating temperature alarm is included. Increased accessibility all around the Mass Spectrometer with a fully movable bench, on lockable casters wheels (ease the instrument service).


Reduce linear space requirement by 30% for the mass spectrometer installation, by integrating all system peripherals into a well-designed IonBenchTM. As an example the control computer, fl at screen monitor can, solvent waste container can be attached conveniently without additional footprint.


Vacuum pumps positioned on a specifi c patented absorbing vibration system to protect turbomolecular pumps by reducing vibration by 99% (this is typically one issue that is not addressed by conventional lab furniture and excessive vibration reduces the performance and lifetime of turbomolecular pumps inside the mass spectrometer).


Better ergonomics and security in labs, by using a bench designed for mass spectrometry applications (solvent storage, increased number of electrical power sockets, fl at screen monitor arm, Printer storage, Auto Sampler, PC Holder)


IonBench LC benches contribute signifi cantly to lab safety and productivity. They are stable, secure platforms that electrically raise and lower stacked HPLC/UHPLC systems. They are large enough to safely and securely accommodate any stacked HPLC/UHPLC system available in the industry. The primary goal of IonBench LC is to enhance safety during routine operation of high pressure liquid chromatographs


IonBench is distributed on line via its dedicated web site, visit www.ionbench.com for further information. 32133pr@reply-direct.com


Benchtop NMR Capabilities Expanded with 31P Phosphorus System


Magritek have expanded the range of their Spinsolve Benchtop NMR spectrometers with the Spinsolve Phosphorus. Key applications include routine purity assessment and reaction monitoring. The Magritek Spinsolve Benchtop NMR spectrometers have repeatedly demonstrated the highest performance in their class in terms of superior sensitivity and resolution. The Spinsolve Phosphorus extends that capability to include the 31P nucleus. 31P is a 100% natural abundance nucleus commonly found in many organic compounds. The high NMR sensitivity of 31P combined with its large chemical shift range, simple spectra, and absence of impurities in the background spectrum make 31P NMR ideal for routine purity assessment and tracking reactions The magnet design and thermal control, together with the internal lock, provide remarkable long term stability which means minimal requirement for optimisation sequences (shimming). Compact and convenient, it is easy to operate and with low cost of entry and maintenance, Spinsolve is a most attractive proposition for laboratories today.


The simplicity of the phosphorus spectrum combined with the high sensitivity of the Spinsolve instrument makes Spinsolve Phosphorus ideal for purity assays. These are illustrated in new literature from Magritek. For example, impurities can be detected at sub 1% levels in a sample of 300mM nucleoside phosphoramidite in deuterated chloroform. This is important due to its use in the synthesis of oligonucleotides. In another example the oxidation reaction of triphenylphosphine to triphenylphoshine sulphide is followed. These chemicals are important in their use to analyse certain sulphur compounds. Of particular note is the clean separation and minimum number of peaks in the spectra which makes monitoring of the reaction straightforward.


Users have found the Spinsolve software platform beautifully simple and straightforward to use due to the clean and intuitive user interface. It incorporates the ability to easily switch between different nuclei offered by the system via simple software command. Scripts are used to automate experiments. A range of script templates are provided for easy user modifi cation. Scripts are displayed graphically to provide a clear picture of the progress of any sequence, a feature which is ideal for monitoring the state of the system during reaction monitoring. It is even possible to switch nuclei inside a reaction monitoring sequence.


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Gas Analysers Feature Broad Pressure Range


High-End Single Quadrupole Gas Chromatograph Mass Spectrometer Released


Shimadzu has released its GCMS-QP2020 high- end single quadrupole gas chromatograph mass spectrometer. With excellent performance and smart operability, the instrument satisfi es a wide range of needs for single quadrupole GC-MS systems. The GCMS-QP2020 achieves the highest sensitivity in its class and enables high-speed performance for many applications.


The new turbomolecular pump with improved exhaust effi ciency provides higher accu racy in analysis, even when hydrogen or nitrogen in


Hiden are exhibiting their latest laboratory gas analysers at Pittcon 2016, 6th - 10th March, Atlanta, GA USA. Hiden Analytical’s QGA systems are suited for direct real- time analysis, quantifi cation and control of gas related processes ranging in pressure from 100 mbar to 30 bar.


The bench-top mass spectrometer systems are coupled to the user process by the integral robust, fl exible, quartz-lined heated capillary with sample consumption rates as low as 1 mL/min and response times as low as 150 milliseconds. Process interface options enable analyses through the very broad pressure regime and are suited to diverse application areas including top-gas analysis, measurement of dissolved species, multi-stream monitoring of gas feed and process exhaust lines (up to 80 individual gas streams), process/thermal reaction studies, respiratory analysis.


System operation, calibration, data acquisition and display are fully automated, with full manual control selectable when required. Integral I/OÆs permit import of external data, such as temperature, for integration with the mass spectral display, and output of process detail for process control functions.


For full details visit the Hiden Booth 3942 at Pittcon 2016, or visit www. HidenAnalytical.com.


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addition to helium is applied as the carrier gas. The GCMS-QP2020 also features a function enabling switching of ionisation modes without stopping the mass spectrometer as well as ultra-fast scan performance, which allows the use of various analytical conditions. The GCMS-QP2020 with Shimadzu’s many specialised databases and application software enables confi gura tions tailored to a multitude of applications and purposes.


The GCMS-QP2020 provides not only high-sensitivity and high-speed performance, but can also be used for a wide range of applications with enhanced, specialised databases designed for specifi c purposes, including the testing/inspection of food, pharmaceuti cal, chemical as well as the environmental applications.


Beyond the GCMS-QP2020, Shimadzu offers the entry model GCMS-QP2010 SE and the fl agship GCMS- TQ8040 triple quadrupole model to satisfy all types of laboratory re quirements.


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INTERNATIONAL LABMATE - JANUARY/FEBRUARY 2016


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