27


Figure 5. HILIC Analytical on 100-60% of B in A for 6 min gradient – Solvent A: Water with 10 mM ammonium formate; Solvent B: 95% ACN in water with 10mM ammonium formate; Atlantis HILIC Silica column 4.6x100mm, 5µm


Figure 6. Flash Chromatography Polar Test Mix on 100-60% of B in A for 9 min gradient – Solvent A: Water with 10 mM ammonium formate; Solvent B: 95% ACN in water with 10mM ammonium formate; Teledyne ISCO 12g GOLD Silica (20-40 µm) Redisep, 30 mlmin-1, 220 nm and 254 nm.


Figure 7. HILIC Analytical on 100-60% of B in A for 6 min gradient – Solvent A: Water with 10 mM ammonium formate; Solvent B: 95% ACN in water with 10mM ammonium formate;


All column dimensions 4.6x100mm, 5µm.


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