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CONFERENCE REVIEW | PLASTIC PIPES IN INFRASTRUCTURE


advanced techniques such as scanning electron microscopy (SEM), gas chromatography-mass spectrometry (GCMS) and nuclear magnetic resonance (NMR). Kalloudis presented several case studies to


illustrate various types of pipe failure, including hot water PVC pipe and PE100 water pipes. Several failures of the PVC pipe had caused a factory shutdown. Some pipe sections were removed and analysed by DSC – which revealed that the PVC’s glass transition temperature had been lowered – as the elevated temperatures had led to thermal relaxation and resulted in physical ageing.


PE100 water pipe butt welds were exhibiting


brittle mode failures, though no problems were identified in the welding process. The problem was identified through micrographs – which revealed large agglomerates of carbon black. This was confirmed using SEM. In a similar case, a butt fusion-welded PE100 pipe showed excessive blistering on the welding surface – though DSC, FTIR and SEM showed nothing suspicious. However, GCMS revealed trace amounts of a saturated hydrocarbon on the


non-heated side of the pipe – leading to the conclusion that diesel had contaminated the PE100 during processing.


As well as using techniques like these to identify


the reasons for failure, Kalloudis said it was vital to implement effective QA and QC programmes. “Although a lot of research has been done in the


production of PE pipe materials, bad QA and QC processes can threaten the pipelines,” he said. “Contractors and utility companies must establish tight QA/QC procedures and follow the require- ments of the relevant standards.” Joaquín Lahoz Castillo, senior pipe researcher at


CEIS in Spain, described three case studies involving failed PVC pressure pipes. “Longitudinal crack failure in large PVC pipes in


irrigation projects have been a recurrent topic in the last few years,” he said. “We wanted to know if this was caused by rapid crack propagation (RCP), or whether it was about pipe quality.” In the first example, PVC pipes from 2008 were found to have longitudinal fissures and cracks. There were noticeable brown and grey particles visible in the cracks. Tests showed onset tempera- tures below 180°C and a gelation degree of 61%.


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