Ultra-Low kV EDS
and work on developing applications for Li analysis in battery materials. Finally, we thank Peter Statham and Philippe Pinard of Oxford Instruments NanoAnalysis for help and advice preparing this paper.
References [1] I Barkshire et al ., Microchimica Acta 132 ( 2000 ) 113 – 28 . [2] P Pinard , unpublished PhD thesis, RWTH Aachen University, 2016.
[3] J Goldstein et al ., Scanning Electron Microscopy and X-ray Microanalysis , T ird Edition , Springer , New York , 2003 .
Figure 12 : Detection of Li K X-rays from lithium-containing compounds used in research on next-generation Li batteries. (a) Li 2 S [ 14 ] and (b) lithium lanthanum zirconate (LLZ). X-ray spectra collected (a) at 2 kV using an 80 mm 2 windowless detector and (b) at 3.5 kV using a 100 mm 2 windowless detector.
[4] S Burgess et al ., Microsc Microanal 19 ( S2 ) ( 2013 ) 1142 – 43 . [5] S Burgess et al ., Microsc Microanal 22 ( S3 ) ( 2016 ) 112 – 13 . [6] F Zhou et al ., Microsc Microanal 22 ( S3 ) ( 2016 ) 1586 – 87 . [7] G Bertali et al ., Microsc Microanal 21 ( S3 ) ( 2015 ) 463 – 64 . [8] J Sagar et al ., Microelectron Reliab 64 ( 2016 ) 367 – 69 . [9] C Lechene et al ., J Biol 5 ( 2006 ) 20 . [10] X Li et al ., Microsc Microanal , late breaking poster, 2012. [11] S Burgess et al ., Microsc Anal (May 2013) S8-13. [12] X Li et al ., Microscopy and Analysis 19 ( S2 ) ( 2013 ) 1136 – 37 . [13] J Goldstein et al ., Scanning Electron Microscopy and X-ray Microanalysis , T ird Edition , Springer , New York , 2003 , chapter 6 and additional CD.
[14] P Hovington et al ., Scanning 38 ( 2016 ) 571 – 78 . [15] H Demers et al ., Microsc Microanal 22 ( S3 ) ( 2016 ) 408 – 09 .
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