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TESTING | MATERIALS


Analysing the composition and properties of polymers, additives, and


compounds is crucial for product development and quality control. Jennifer Markarian finds that test methods are evolving for compostable compounds


Advances in materials analysis technology


Materials testing is essential for both developing and ensuring production quality of plastics compounds. Analytical equipment companies continue to develop user-friendly and automated features that bring the power of high-tech analysis to a broader user group, providing new tools for analysing polymers, additives and contaminants. Thermal analysis techniques – including differen- tial scanning calorimetery (DSC), simultaneous thermal analysis (STA), thermomechanical analysis (TMA) and dynamic mechanical analysis (DMA) – are widely used in polymer industries to identify polymers, quantify impurities, evaluate crystallinity, measure mechanical properties, and troubleshoot production issues, said Terri Chen, Director of Business Development at Cannon Instrument. “However, certain thermal measurement results can be difficult to under- stand,” said Chen. “In these cases, great strides are gained by adding a real-time image or video capability, leading to a better understanding of the analytical results. In recent


www.compoundingworld.com


years, more researchers have moved toward combining a visual/imaging capability with their analytical tools.” Last year, Cannon began partnering with Hitachi


High-Tech, and the companies are collaborating to grow Hitachi’s thermal analysis business in the US, said Chen. The Hitachi DSC-RealView system offers real-time visual capabilities integrated with thermal analysis equipment (DSC, STA and DMA). “Being able to visualise the changes of the sample during a thermal measurement can elucidate unexpected testing results by supplying supplemental information regarding the sample under test,” ex- plained Chen. “For example, in a DSC measurement, the Hitachi DSC-RealView system can capture images or record videos during the measure-


IMAGE: HITACHI


ment, which allows identifying and interpreting any fake transi- tions. When testing crystalline polymers with the Hitachi DSC, the real-time observation allows re- searchers to better understand


March 2025 | COMPOUNDING WORLD 37


Main image: Sample tray in Mettler Toledo’s new DSC 5+ test instrument with MultiStar sensor


technology


Left: Hitachi NEXTA DSC with polarised microscope


IMAGE: METTLER TOLEDO


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