MATERIALS | TESTING
Right: Instron has supplied a testing system from its 5900 series to NPL in the UK to develop a new through- thickness composite testing standard
Source (TPS) methods allows unbiased exploration if a material exhibits these properties.” He says the ability to replicate environments that
affect thermal transport properties is also important. “From harsh environments of a cold
winter (-50℃) to the melt phase of a polymer (200-300℃) there can be drastic changes in thermal conductivity. With environmental control
chambers and speciality testing cells, real-world testing of thermal conductivity in these environments can be accomplished.” There are also particular challenges in
measuring and characterising the thermal properties of thin films. “As a material enters the range below 0.5mm, its inherent thermal properties can change – meaning traditional test methods that require larger or thicker samples do not present relevant data. With the TPS thin film module on Trident, understanding of a material’s thermal conductivity at this thickness can be developed,” Nickerson says. C-Therm’s flagship instrument, Trident, was
introduced to provide a thermal conductivity testing solution that brings together the most prominent methods for polymer testing - MTPS for rapid testing, double-sided TPS for testing thin films, and TLS (Needle Transient Line Source) needle probes for testing of polymers in their melt phase. The company says that MTPS is fast, easy and highly accurate, using a single-sided, ‘plug & play’ sensor suitable for testing solids, liquids, powders and pastes. Applications include pure and composite polymers, rubber and 3D anisotropic samples. TPS uses a flexible double-sided sensor that can provide greater control over experimental parameters, making it suitable for more advanced users. Applications include anisotropic polymers and thin films. The TLS Needle sensor offers maximum robustness and can be applied in polymer melts and plastics injection moulding.
Composite standard Testing systems maker Instron has recently participated in a collaborative test programme led by the National Physical Laboratory (NPL) in the UK to support development of a new ISO standard for through-thickness testing of polymer composite materials. The new standard, ISO NP 20975-1 (Fibre-Reinforced Plastic Composites - Determination of Laminate Through-Thickness Properties, Part 1: Specimen Designs for Direct Tension and Compression Tests), covers both tension and compression testing in the through- thickness direction. Composite materials are most commonly tested
36 COMPOUNDING WORLD | January 2022
to determine their in-plane properties. However, there is an increasing demand for measurement of their through-thickness properties in the development of reinforcements. The test programme involved the use of an
Instron 5985 electromechanical testing system with 250kN capacity. The tensile test specimens were supplied with bonded metal studs, which were gripped between a pair of Instron hydraulic grips, which had been precisely aligned using an AlignPRO fixture and checked using a strain gauged alignment specimen. The compression test specimens were tested between a pair of compression platens mounted on the hydraulic grips. The upper compression platen incorporated a lockable spherical seat which allowed the alignment of the platens to be adjusted. For strain measurement, four axial and four
transverse strain gauges were used (for determining Poissons ratio). The gauges were connected using Instron strain gauge adapters and an expansion channel module. Test control, data collection and analysis were performed using Bluehill Universal software. Successful tests were carried out on both carbon and glass fibre specimens. The company says the data will help to validate and establish the precision of the new test method.
CLICK ON THE LINKS FOR MORE INFORMATION: �
www.intertek.com �
www.perkinelmer.com �
www.tainstruments.com �
www.dynisco.com �
www.ctherm.com �
www.instron.com
www.compoundingworld.com
IMAGE: INSTRON
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