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Table of Contents


Chapter 12 Fast Separations of Phytochemicals by High- performance Liquid Chromatography Using Monolithic Columns


Mauricio A. Rostagno and Ana Villares 12.1 Introduction


12.4 Practical Aspects and Considerations for the Use of Monolithic Columns


12.5 Method Development Strategies Using Monolithic Columns


12.6 Future Potential of Monolithic Columns in Liquid Chromatography


References


Chapter 13 Monolithic Stationary Phases for Affinity-based Separations


Panagiotis Manesiotis and Georgios Theodoridis 13.1 Introduction


13.2 Monolithic Materials for Affinity Chromatography


ix


339 339


12.2 Chromatographic Characteristics of Monolithic Columns 341 12.3 Applications of Monolithic Columns for the Analysis of Phytochemicals


343 366 368 376


377


381 381


13.3 Applications of Monoliths in Affinity Chromatography 387 13.4 Molecularly Imprinted Polymers 13.5 Concluding Remarks References


Chapter 14 Immobilisation of Enzymes on Monolithic


Matrices: Applications in Drug Discovery 403 Vincenza Andrisano and Manuela Bartolini 14.1 Introduction


14.2 Enzyme Immobilisation on Monolithic Matrices


403 405


14.3 Determination of Enzyme Activity After Immobilisation 412 14.4 Kinetic Characteristics of the Immobilised Enzyme 14.5 Enzyme Inhibition 14.6 Conclusions References


415 417 423 423


383 392


399 400


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